The works of the highly experienced and famous chymist, John Rudolph Glauber, Volume 1 Papyras Classics

← The works of the highly experienced and famous chymist, John Rudolph Glauber, Volume 1

Chapter 54

Point III

The volatile and immature Marcasites of Sol and Luna are fixed in the space of three hours, so that they render a double quantity of Metal, to what they could have done before fixation, &c.

This fixation is a singular secret, in perfecting Antimonial and Arsenical Minerals, which are wholly crude, which commonly yield a little Gold: For when Minerals contain much Antimony, Arsenick, or Orpiment, and are torrefied in the common way, then the Arsenick or Orpiment destroyeth much of the Gold, carrying it away in fume; but if they be melted without a foregoing torrefaction, then the blowing forceth away more; if from a Mineral of this sort, the yellow or red Sulphur, Arsenick, or other rapacious substances, be diminished or consumed, by closing it in Earthen Vessels, as many do, then by this means the Mineral is burnt, loseth its flux and ingress into Lead, so that much of the gold is destroyed, and reduced into Scoria; to prevent which, this following way is the best: With one part of the mineral mix half a part of Nitre, let it be kindled with a Coal, and fixed, then the Nitre burneth away the greatest part of the rapacious sulphur, and fixeth the rest, so that there is but little of the Gold lost, and it keepeth its flux and ingress into Lead; if it be put into the foregoing Furnace, and there wrought, it yieldeth all the gold and silver which it containeth, and nothing is lost. Here some may object, and say, That although in this manner, more gold may be obtained; yet the Nitre maketh the work dear, which I indeed confess to be true, if the Nitre be bought at a dear rate, but if by an artificial Culture, it may alwaies be had at hand, it will cost little, and this torrefaction and fixation, may be perfected with great profit.

Point IV.

All Gold and Silver not purely melted from its Marcasite, may be swiftly purged from every Additament, the silver separated from the Gold, by fusion only, with a small labour and cost, but in great weight.

This way of purifying ☉ and ☽ from all addition quickly, and in an easie manner, is a thing most profitable, and an Art highly necessary to be known by those who handle metals; for it is sooner done, than by the way of cupellating or blowing off with Lead, but is dearer, by reason of the Nitre; nevertheless, the labour is easie and pleasant, and it is done in this manner: Let a Crucible of impure gold or silver be placed in such a Furnace as is described and depicted in the Fourth Part of our Furnaces, let it be melted, then cast in some Regulus of Antimony, more or less, according to the greater or lesser impurity of the Gold, and according as it hath more or less need of cleansing for its purification. When all shall flow and be clear in the Crucible, cast into the Crucible upon the metal, at several times, about so much Nitre, as there is of addition to the Gold; let it flow, then the Nitre attracteth the Regulus of Antimony, together with the impurity contained in the Gold, which passeth into Scoria. And this Process doth not serve only for impure Sol and Luna, but also for such Sol and Luna which contain Copper, Iron, Lead, Tin, Chalcitis, Aurichalcum, and other metallick and mineral matters, Tin especially, which is difficult to be separated from Sol and Luna by Lead, without loss. But in this manner it may be quickly and easily done. But that my meaning may be the more rightly understood and the less errour be committed in working, I will here institute the Process clearly, and in express words. Suppose to ℔ j. of gold or silver, there be two lothones of Copper, and three lothones of Tin (a lothone is half an ounce) which I would separate, and if it be done by the known way of blowing off with Lead, there will need at the least thirty or forty lothones of Lead, and nevertheless one part of the Sol or Luna will be lost; but by my way to two lothones of Copper, and three lothones of Tin, adjoin five lothones of Regulus of Antimony, then abstract the Regulus, together with the addition of Copper and Tin, by the mediation of Nitre, which may be done in the Crucible in the space of one hour, which by torrefaction and agitation in the common way, could scarcely have been done in 10 or 12 hours; besides nothing of the Additaments is lost, all remaineth in the Scoria, from which, afterwards, as well the ♃ as the ♀ and Regulus of Antimony may be recovered, to wit, if the Scoria, in which the ♃, ♀, and Regulus of Antimony is, be put into a Crucible, a live Coal cast in, and then the Crucible covered with a tyle, let them flow a quarter of an hour, pour all out, and you shall find in the bottom of the Cone a little Regulus, in which will be the remaining Sol or Luna, which the Scoria did prey upon; let them be depurated on a Cupel, if they be not already pure enough: The Scoria being again melted, cast in a live Coal, suffer all to flow well together, again there will fall another Regulus from the Copper, the ♃ & ♂ remaineth, and neither by Coals nor any other art, can be brought into Regulus; but if these Scoria be driven through a probatory Furnace, then they also yield the Tin again, and that better than it was before. This Process is not only pleasant, artificial, swift and easie, by which gold and silver is quickly and purely separated from all addition, but there is also hidden in it a great mystery: But because I have only proposed to prove those things to be true and natural, of which I have made mention in my Miraculum Mundi, let what I have now said suffice, and what is here desir’d may be found perspicuously and satisfactorily declared in the following Processes.